Dean And Stark Apparatus
Dean And Stark Apparatus

Dean And Stark Apparatus

Price 7500.0 INR/ Piece

MOQ : 1 Piece

Dean And Stark Apparatus Specification

  • Measuring Range
  • 0-100 ml or as per receiver volume
  • Max Height
  • Glassware height up to 500 mm depending on flask size
  • Automation Grade
  • Manual
  • Application
  • Determination of water content in solvents, oils, emulsions; azeotropic distillation
  • Port Size
  • 24/29 (neck joint); receiving tube volume: 2-100 ml as per setup
  • Specimen Size
  • Depends on flask size (commonly 100 ml - 2 Litres)
  • Hardness
  • 7 Mohs (borosilicate glass)
  • Display Type
  • Graduated glass receiver
  • Response Time
  • Immediate (visual observation)
  • Mounting Type
  • Tabletop with support stand/clamp
  • Resolution
  • 0.1 ml
  • Power Supply
  • Not required (runs without electricity)
  • Accuracy
  • 0.1 ml (depending on receiver tube graduation)
  • Features
  • Borosilicate glass, leakproof joints, accurate graduations, chemical resistance
  • Temperature
  • Up to 250C (commonly used with heating mantle or oil bath)
  • Interface Type
  • Glassware joints; manual operation
  • Number of Specimens
  • Single per setup
  • Equipment Type
  • Dean and Stark Apparatus
  • Usage
  • Laboratory chemical analysis, moisture determination
  • Capacity
  • Typically 50 ml, 100 ml, 250 ml (receiver tube); flask up to 2 Litres
  • Machine Weight
  • Depends on capacity (typically 500-1000 g for standard setup)
  • Control Mode
  • Manual
  • Working Principle
  • Solvent-water azeotropic distillation and collection
  • Joint Type
  • Standard tapered (24/29, 19/26, or as required)
  • Azeotrope Collector Volume
  • 2 ml to 250 ml
  • Receiver Tube Graduations
  • Clear, etched, solvent resistant
  • Corrosion Resistance
  • High (suitable for most laboratory solvents)
  • Flask Compatibility
  • Round bottom flasks, capacity 100 ml to 2 L
  • Compliance
  • ISO 3585, ASTM D95
  • Material
  • Borosilicate glass, PTFE stopcock (optional)
  • Heat Source Compatibility
  • Heating mantles, oil baths, hot plates
 

Dean And Stark Apparatus Trade Information

  • Minimum Order Quantity
  • 1 Piece
  • Supply Ability
  • 500 Pieces Per Month
  • Delivery Time
  • 7 Days
 

About Dean And Stark Apparatus

The Dean and Stark Apparatus is a specialized laboratory glassware setup used for the determination of water content in various substances through azeotropic distillation. It is widely employed in chemical, petroleum, and food industries for accurate moisture analysis, particularly in oils, bitumen, and organic compounds.

The apparatus works by separating water from a sample using an immiscible solvent, typically through reflux distillation. The collected water is then measured in a calibrated receiver, providing precise and reliable results.

Key Features:

  • Accurate moisture determination by azeotropic distillation
  • Made from high-quality borosilicate glass for durability and thermal resistance
  • Clear and precise calibration markings
  • Resistant to chemicals and high temperatures
  • Easy assembly and operation
  • Available in different capacities and configurations

Applications:

  • Petroleum and oil testing laboratories
  • Chemical and pharmaceutical industries
  • Food processing and quality control
  • Research and educational laboratories
  • Bitumen and asphalt testing

Technical Specifications (Typical):

  • Material: Borosilicate Glass
  • Capacity: 5 ml, 10 ml, 25 ml receiver (customizable)
  • Joint Size: Standard ground glass joints
  • Method: Azeotropic distillation
  • Compatibility: Suitable for organic solvents like toluene or xylene

Packaging Details:
Carefully packed in protective materials to prevent breakage during transit.

Usage Instructions:

  1. Assemble the apparatus with flask, condenser, and receiver.
  2. Add sample and solvent into the distillation flask.
  3. Heat the mixture to initiate distillation.
  4. Collect and measure separated water in the calibrated receiver.

Safety & Maintenance:

  • Handle glassware carefully to avoid breakage
  • Use in a well-ventilated area
  • Clean thoroughly after each use
  • Avoid sudden temperature changes to prevent cracking


Reliable Water Content Determination

Accurately measure water content in oils, solvents, and emulsions using the Dean and Stark Apparatus. Engineered for laboratory chemical analysis, its borosilicate glass construction and solvent-resistant features ensure precise and repeatable results, essential for quality and compliance in testing protocols.


Flexible, Manual Operation for Every Lab

The apparatus requires no electricity and is designed for ease of use on laboratory workbenches. Its versatility is demonstrated by compatibility with a range of flask volumes and receiver tube capacities. Standard joint sizes and leakproof design guarantee secure connections and straightforward sample handling.


Built to Last: Chemical and Thermal Durability

With high resistance to corrosion and temperatures up to 250C, this equipment supports rigorous laboratory processes. The clear graduations and chemical-resistant materials provide durability, safety, and minimal maintenance, making it a reliable tool for frequent laboratory use.

FAQ's of Dean And Stark Apparatus:


Q: How does the Dean and Stark Apparatus determine water content in samples?

A: The apparatus operates through azeotropic distillation, where the sample is heated with a suitable solvent to co-distill water. The water separates and is collected in a graduated receiver tube, allowing precise measurement of moisture content.

Q: What types of samples and chemicals can be analyzed using this apparatus?

A: It is suitable for analyzing a wide range of samples, including oils, organic solvents, and emulsions. The borosilicate glass and chemical-resistant components allow it to withstand most laboratory solvents commonly used for moisture determination.

Q: When should I select a particular receiver tube volume or flask size?

A: Receiver tube volume (2-250 ml) and flask size (100 ml-2 L) should be chosen based on your sample volume and expected water content. For higher moisture samples, larger receiver tubes and flasks are recommended to accommodate the distillation process efficiently.

Q: Where can the Dean and Stark Apparatus be used in the laboratory?

A: This apparatus is typically used on a stable benchtop setup, secured with a support stand or clamp. Its design is optimized for laboratory environments, making it ideal for research, quality control, industrial analysis, and educational laboratories.

Q: What is the process for using the Dean and Stark Apparatus?

A: After assembling the apparatus with the appropriate flask and receiver, the sample and azeotroping solvent are added. The mixture is heated (using a mantle, oil bath, or hot plate), causing water to distill and collect in the receiver, which can be read immediately via the graduated scale.

Q: What benefits does the apparatus offer over automated moisture meters?

A: The Dean and Stark Apparatus provides direct measurement, immediate visual feedback, and does not require electricity or complex calibration. Its high chemical and thermal resistance ensures reliability and minimal risk of interference from sample matrix effects.

Q: How accurate are the measurements, and how is resolution ensured?

A: With clear, finely etched graduations on the receiver tube and careful manual operation, the apparatus typically offers a measurement resolution of 0.1 ml, making it highly suitable for precise laboratory moisture determinations.

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